CAS No.103-01-5,Glycine,N-phenyl- Suppliers,MSDS download

Products Categories

Pharmaceutical (102)
Organic Chemicals (33)
Others (26)
Reagent (7)
Materials (4)
Dyestuff and Pigment (3)
Catalyst and Auxiliary (1)

Basic Information

Molecular Structure:
CAS No.:	103-01-5
Name:	Glycine,N-phenyl-
Article Data:	101
Cas Database

Formula:	C₈H₉NO₂
Molecular Weight:	151.165
Synonyms:	H-DL-Phg-OH;TR-NPG;(Phenylamino)aceticacid;Acetic acid, (phenylamino)-;Anilinoacetic acid;N-(Phenylamino)aceticacid;N-Phenylglycine;NSC 83567;
EINECS:	203-070-2
Density:	1.259 g/cm³
Melting Point:	121-127 °C
Boiling Point:	359 °C at 760 mmHg
Flash Point:	170.9 °C
Solubility:	moderately soluble in water
Appearance:	ochre to yellow-brown fine powder
Hazard Symbols:	N/A
Risk Codes:	36/37/38
Safety:	22-24/25
Transport Information:	N/A
PSA:	49.33000
LogP:	1.25610

Synthetic route

: 105-36-2
ethyl bromoacetate

: 62-53-3
aniline

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
Stage #1: ethyl bromoacetate; aniline With silica gel at 20℃; for 0.116667h; microwave irradiation; Stage #2: With sodium hydroxide In ethanol for 0.166667h; Heating;	93%
Stage #1: ethyl bromoacetate; aniline With potassium carbonate for 1.5h; Milling; Stage #2: With potassium hydroxide for 1.5h; Milling;	91%
Stage #1: ethyl bromoacetate; aniline Stage #2: With sodium hydroxide

: 21969-70-0
2-anilinoacetamide

: 71-36-3
butan-1-ol

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
	90%

: 65171-67-7
tert-butyl 2-(phenylamino)acetate

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
With trifluoroacetic acid In dichloromethane for 3h;	90%
In water; isopropyl alcohol at 200℃; for 0.25h; Solvent; Temperature; Flow reactor;	77%

: 591-50-4
iodobenzene

: 56-40-6
glycine

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 75 - 80℃; for 72h;	87%
With copper(l) iodide; 2-(2-methyl-1-oxopropyl)cyclohexanone; caesium carbonate In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere;	82%
With copper(I) oxide; caesium carbonate at 100℃; for 0.666667h; Sealed tube; Microwave irradiation;	10%

: 108-86-1
bromobenzene

: 56-40-6
glycine

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
With copper(l) iodide; 2-(2-methyl-1-oxopropyl)cyclohexanone; potassium carbonate In water at 90℃; for 0.833333h; Microwave irradiation; Green chemistry;	81%
With pectin-stabilized copper nanoparticles In dimethyl sulfoxide at 110℃; for 2h;	71%
With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 90℃;	62%
With copper(l) iodide; potassium carbonate In N,N-dimethyl acetamide at 90℃;

: 2216-92-4
N-phenylglycine ethyl ester

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
With sodium hydroxide In water for 0.5h; Heating;	73%
With sodium hydroxide for 0.5h; Heating;	70%
Stage #1: N-phenylglycine ethyl ester With sodium hydroxide In water for 0.5h; Reflux; Stage #2: With hydrogenchloride In water pH=2;

: 178695-68-6, 181121-53-9
1-phenyl-4-oximinoimidazolidine

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
With hydrogenchloride Hydrolysis;	60%

: 591-50-4
iodobenzene

: 556-50-3
glycylglycine

A: 852380-00-8
N-(N-phenyl-glycyl)-glycine

B: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
With potassium phosphate; copper(l) iodide; 2-(N,N-dimethylamino)ethanol In water at 70℃; for 16h;	A 40% B 27%

...Expand

: 1457-85-8
Ethyl oxanilate

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
With sulfuric acid Electrolysis.elektrolytische Reduktion;

: 622-14-0
N,N'-diphenylmethylenediamine

: 103-01-5
N-Phenylglycine

Conditions

Conditions	Yield
With potassium cyanide; ethanol

Total:133 Page 1 of 4 1 2 3 4 Next>>

Please post your buying leads,so that our qualified suppliers will soon contact you!
*Required Fields

Chemistry

The molecular formula of N-phenylglycine(103-01-5) is C₈H₉NO₂ and its formula weight is 151.16.
N-phenylglycine(103-01-5) has a melting point of 121-123 °C(lit.).
The chemical synonyms of N-phenylglycine(103-01-5) are AURORA KA-3653;ANILINOACETIC ACID;H-PHENYLGLY-OH;AKOS B003332;RARECHEM AL BO 1139;N-PHENYLGLYCIN;N-PHENYLGLYCINE;N-PHENYL-GLY-OH
The molecular structure of N-phenylglycine(103-01-5):

Toxicity Data With Reference

RTECS#: CAS# 103-01-5: None listed
LD50/LC50: RTECS: Not available.
Carcinogenicity: N-PHENYLGLYCINE, 93%(TLC) - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
Other: The toxicological properties have not been fully investigated.

Safety Profile

Safety Statements 22-24/25
WGK Germany 3
HS Code 29224995

Specification

Chemical Stability: Stable under normal temperatures and pressures.
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents.
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, irritating and toxic fumes and gases, carbon dioxide, nitrogen.
Hazardous Polymerization Has not been reported.