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1072-53-3

Basic Information
CAS No.: 1072-53-3
Name: 1,3,2-Dioxathiolane,2,2-dioxide
Article Data: 48
Cas Database
Molecular Structure:
Molecular Structure of 1072-53-3 (1,3,2-Dioxathiolane,2,2-dioxide)
Formula: C2H4 O4 S
Molecular Weight: 124.117
Synonyms: Ethyleneglycol, cyclic sulfate (8CI); Ethylene sulfate (((CH2O)2SO2)) (6CI,7CI);1,2-Ethylene sulfate; Ethylene sulfate; NSC 526594
EINECS: 600-809-4
Density: 1.604 g/cm3
Melting Point: 95-97 °C(lit.)
Boiling Point: 231.1 °C at 760 mmHg
Flash Point: 93.5 °C
Solubility: N/A
Appearance: yellowish crystal
Hazard Symbols: N/A
Risk Codes: 22
Safety: Questionable carcinogen with experimental tumorigenic and neoplastigenic data. Mutation data reported. When heated to decomposition it emits toxic fumes of SOx. See also SULFATES and ESTERS.
Transport Information: N/A
PSA: 60.98000
LogP: 0.35880
Synthetic route
75-21-8

oxirane

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With cerium(IV) oxide; iron(III) chloride; sulfur dioxide; antimony(III) chloride at 140℃; under 45004.5 Torr; for 2h; Pressure; Temperature; Inert atmosphere; Autoclave;97.8%
With aminosulfonic acid; acetic anhydride at -10 - 20℃; for 24h; Autoclave;73.22%
107-21-1

ethylene glycol

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With fluorosulfonyl fluoride; N,N,N,N,-tetramethylethylenediamine In acetonitrile at 60℃; for 36h; Reagent/catalyst; Solvent; Temperature;96.5%
Stage #1: ethylene glycol With fluorosulfonyl fluoride; sodium sulfate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide In tert-butyl methyl ether at 5 - 10℃; for 1h; Autoclave;
Stage #2: With 15-crown-5; 18-crown-6 ether In dichloromethane Solvent; Reagent/catalyst; Temperature;
81.8%
With potassium hydroxide; sulfuryl dichloride; silica gel 1.) reflux; 2.) rt., 3 h; Yield given. Multistep reaction;
Stage #1: ethylene glycol With potassium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene at 130 - 140℃; for 20h;
Stage #2: With fluorosulfonyl fluoride In acetonitrile at -15 - -5℃; for 1h; Temperature; Reagent/catalyst; Solvent; Sealed tube; Inert atmosphere;
106.3 g
With sulfuryl dichloride In chloroform at 5 - 60℃; for 3h;375 g
3741-38-6

ethylene sulfite

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With manganese(IV) oxide In water at 5℃; for 0.75h; Reagent/catalyst; Temperature;95.84%
With sodium hydrogencarbonate; iron(II) sulfate In dichloromethane pH=7 - 8; Concentration;90.66%
With ruthenium trichloride; calcium hypochlorite at 15℃;83%
74-85-1

ethene

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With PhI(1+)OSO2O(1-) In dichloromethane at 15℃; for 0.3h;85%
With μ-oxodiphenyldiiodine(III) sulfate; phenyliodine(III) sulfate Yield given;
96-49-1

[1,3]-dioxolan-2-one

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With carbon dioxide; sulfur trioxide at 25 - 65℃; for 8h; Inert atmosphere;76%
7719-09-7

thionyl chloride

107-21-1

ethylene glycol

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
Stage #1: thionyl chloride; ethylene glycol at 25 - 30℃; for 3h; Inert atmosphere;
Stage #2: With sodium hypochlorite; ruthenium(III) chloride trihydrate at 0 - 10℃; for 3h; pH=7-8; Concentration; Temperature;
74%

C2H5ClO3S

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With sodium periodate; ruthenium(III) chloride trihydrate In water; acetonitrile for 0.25h; Cooling with ice; Inert atmosphere;70%
106-93-4

ethylene dibromide

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With silver sulfate; xylene
With silver sulfate In xylene
3741-38-6

ethylene sulfite

ruthenium (IV) oxide dihydrate

1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With sodium hypochlorite In dichloromethane; isopropyl alcohol
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
Stage #1: potassium ethyleneglycolate With sulfuryl dichloride In dichloromethane at -10 - 10℃; for 2h; Inert atmosphere;
Stage #2: With 18-crown-6 ether In toluene at 20℃; for 1h; Reagent/catalyst; Solvent;
37.9 g
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Chemistry

IUPAC Name: 1,3,2-Dioxathiolane 2,2-dioxide
The MF of 1,3,2-Dioxathiolane 2,2-dioxide (CAS NO.1072-53-3) is C2H4O4S.

                                         
The MW of 1,3,2-Dioxathiolane 2,2-dioxide (CAS NO.1072-53-3) is 124.12.
Synonyms of 1,3,2-Dioxathiolane 2,2-dioxide (CAS NO.1072-53-3): Ethylene glycol, cyclic sulphate ; 1,3,2-Dioxathiolane 2,2-dioxide ; Sulfuric acid, cyclic ethylene ester
Product Categories: Biphenyl & Diphenyl ether;Heterocyclic Compounds;Heterocyclic Building Blocks;Others;S-Containing
Index of Refraction: 1.469 
Density: 1.604 g/ml 
Flash Point: 93.5 °C 
Boiling Point: 231.1 °C
Melting Point: 95-97 °C
Storage temp: 2-8 °C

Production

Raw materials: Xylene-->1,2-Dibromoethane-->Silver sulfate

Toxicity Data With Reference

1.    

mmo-sat 1 µmol/plate

    CBINA8    Chemico-Biological Interactions. 19 (1977),241.
2.    

hma-mus/sat 5 mmol/kg

    CBINA8    Chemico-Biological Interactions. 19 (1977),241.

Consensus Reports

EPA Genetic Toxicology Program.

Safety Profile

Questionable carcinogen with experimental tumorigenic and neoplastigenic data. Mutation data reported. When heated to decomposition it emits toxic fumes of SOx. See also SULFATES and ESTERS.Safety information of 1,3,2-Dioxathiolane 2,2-dioxide (CAS NO.1072-53-3):
WGK Germany  3
RTECS  JH4800000