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24389-25-1

Basic Information
CAS No.: 24389-25-1
Name: Phosphorodifluoridic acid, lithium salt
Article Data: 3
Cas Database
Molecular Structure:
Molecular Structure of 24389-25-1 (Phosphorodifluoridic acid, lithium salt)
Formula: F2HO2P.Li
Molecular Weight: 107.91
Synonyms: Lithium Difluorophosphate;lithium phosphorodifluoridate;Li difluorophosphate;
EINECS: N/A
Density: N/A
Melting Point: N/A
Boiling Point: N/A
Flash Point: N/A
Solubility: N/A
Appearance: N/A
Hazard Symbols: N/A
Risk Codes: N/A
Safety:
Transport Information: N/A
PSA: 49.94000
LogP: 1.46400
Synthetic route
14456-60-1

difluorophosphoric acid anhydride

lithium fluoride

24389-25-1

difluorophosphinic acid lithium salt

Conditions
ConditionsYield
In neat (no solvent) byproducts: POF3; LiF was added to P2O3F4 at -0.1°C, warmed to ambient temp.; evapd. at 100-120°C;

hexafluorophosphoric acid

16752-60-6

phosphorus pentoxide

lithium fluoride

24389-25-1

difluorophosphinic acid lithium salt

Conditions
ConditionsYield
at 220℃; for 122h; Autoclave;
21324-40-3

lithium hexafluorophosphate

554-13-2

lithium carbonate

24389-25-1

difluorophosphinic acid lithium salt

Conditions
ConditionsYield
at 65℃; for 12h; Temperature; Inert atmosphere; Glovebox;
24389-25-1

difluorophosphinic acid lithium salt

BF8O8P4(1-)*H(1+)

BF8O8P4(1-)*Li(1+)

Conditions
ConditionsYield
In dichloromethane Inert atmosphere;95%

hydroxide

24389-25-1

difluorophosphinic acid lithium salt

(monofluorophosphate)(2-)

Conditions
ConditionsYield
With lithium hexafluorophosphate In water Kinetics; byproducts: F(1-), H2O; stirred at 0.5-32.8°C; excess of Li(1+) supplied by lithium hexafluorophosphate addn.; react. mixt. were taken in certain time intervals, transferred into an ice-cooled quartz flasks and back-titrated immediately with 0.0585 N soln. of HCl;
110-86-1

pyridine

21324-40-3

lithium hexafluorophosphate

24389-25-1

difluorophosphinic acid lithium salt

2,4,6-trivinylcyclotriboroxane*pyridine complex

C2H3BF4O2P(1-)*Li(1+)*5C5H5N

Conditions
ConditionsYield
Stage #1: pyridine; 2,4,6-trivinylcyclotriboroxane*pyridine complex at 20℃; Inert atmosphere;
Stage #2: lithium hexafluorophosphate; difluorophosphinic acid lithium salt at 40℃; for 6h; Inert atmosphere;
17.38 g
3262-89-3

triphenylboroxine

96-49-1

[1,3]-dioxolan-2-one

21324-40-3

lithium hexafluorophosphate

24389-25-1

difluorophosphinic acid lithium salt

C6H5BF4O2P(1-)*Li(1+)*5C3H4O3

Conditions
ConditionsYield
Stage #1: triphenylboroxine; [1,3]-dioxolan-2-one at 20℃; Inert atmosphere;
Stage #2: lithium hexafluorophosphate; difluorophosphinic acid lithium salt at 40℃; for 6h; Inert atmosphere;
20.23 g
96-49-1

[1,3]-dioxolan-2-one

21324-40-3

lithium hexafluorophosphate

24389-25-1

difluorophosphinic acid lithium salt

823-96-1

Trimethylboroxine

CH3BF4O2P(1-)*Li(1+)*5C3H4O3

Conditions
ConditionsYield
Stage #1: [1,3]-dioxolan-2-one; Trimethylboroxine at 20℃; Inert atmosphere;
Stage #2: lithium hexafluorophosphate; difluorophosphinic acid lithium salt at 40℃; for 6h; Inert atmosphere;
18.37 g
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    LiDFP Phosphorodifluoridic acid, lithium salt(CAS No. 24389-25-1) Application:LiDFP Phosphorodifluoridic acid, lithium salt(CAS No. 24389-25-1)

    Shandong Yanshuo Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemi

  • Shandong Yanshuo Chemical Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86 18678179670

    Address:No.19, No.4 Building, Excellent Plasticizing Zone, Qilu International Plasticizing City, Linzi District

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