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30507-70-1

Basic Information
CAS No.: 30507-70-1
Name: 9,12-Tetradecadien-1-ol,1-acetate, (9Z,12E)-
Article Data: 24
Cas Database
Molecular Structure:
Molecular Structure of 30507-70-1 (9,12-Tetradecadien-1-ol,1-acetate, (9Z,12E)-)
Formula: C16H28 O2
Molecular Weight: 252.397
Synonyms: 9,12-Tetradecadien-1-ol,acetate, (9Z,12E)- (9CI); 9,12-Tetradecadien-1-ol, acetate, (E,Z)- (8CI);(Z,E)-9,12-Tetradecadienyl 1-acetate; (Z,E)-9,12-Tetradecadienyl acetate;(Z,E)-9,12-Tetradecadienyl acetate; 9Z,12E-Tetradecadienyl acetate; Litlure B;Prodenialure B; cis-9,trans-12-Tetradecadien-1-ol acetate;cis-9,trans-12-Tetradecadien-1-yl acetate; cis-9,trans-12-Tetradecadienylacetate
EINECS: N/A
Density: 0.89g/cm3
Melting Point: N/A
Boiling Point: 334.8°Cat760mmHg
Flash Point: 102.3°C
Solubility: N/A
Appearance: N/A
Hazard Symbols: N/A
Risk Codes: N/A
Safety: Moderately toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating vapors.
Transport Information: N/A
PSA: 40.13000
LogP: 3.76960
Synthetic route
42521-46-0

Tetradeca-cis-9,trans-12-dien-1-ol

75-36-5

acetyl chloride

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

Conditions
ConditionsYield
With pyridine In tetrahydrofuran93%
42521-46-0

Tetradeca-cis-9,trans-12-dien-1-ol

108-24-7

acetic anhydride

A

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

B

58257-52-6

(Z)-undec-9-en-1-ol

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 18h; Inert atmosphere; chemoselective reaction;A 89%
B n/a
71394-01-9

(E)-12-tetradec-9-yn-12-en-1-yl acetate

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

Conditions
ConditionsYield
With hydrogen; sodium tetrahydroborate; nickel diacetate; ethylenediamine In ethanol Ambient temperature;85%
With quinoline; hydrogen; Lindlar's catalyst In hexane at -10℃;55.5%
With hydrogen; P-2Ni
With quinoline; hydrogen; Lindlar's catalyst In hexane at -10℃; Yield given;
70654-44-3

(Z,E)-9,12-tetradecadien-1-ol

108-24-7

acetic anhydride

A

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

B

70654-47-6

(9E,12E)-tetradeca-9,12-dien-1-yl acetate

C

51354-22-4

(Z,Z)-9,12-tetradecadienyl acetate

D

31654-77-0

(9E,12Z)-9,12-tetradecadienyl acetate

Conditions
ConditionsYield
In pyridineA n/a
B 83%
C n/a
D n/a
112464-06-9

1-<(tetrahydro-2H-pyran-2-yl)oxy> 9Z, 12E-tetradecadiene

75-36-5

acetyl chloride

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

Conditions
ConditionsYield
With pyridine In acetic acid for 12h; Ambient temperature;79.3%
With pyridine; acetic acid72%
112464-06-9

1-<(tetrahydro-2H-pyran-2-yl)oxy> 9Z, 12E-tetradecadiene

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

Conditions
ConditionsYield
acetylation;79%
Multi-step reaction with 2 steps
1: TsOH / methanol / Heating
2: pyridine
View Scheme
Multi-step reaction with 2 steps
1: cc HCl / methanol / 5 h / Ambient temperature
2: 97 percent Chromat. / 4-dimethylaminopyridine / triethylamine
View Scheme
112464-06-9

1-<(tetrahydro-2H-pyran-2-yl)oxy> 9Z, 12E-tetradecadiene

108-24-7

acetic anhydride

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

Conditions
ConditionsYield
With titanium tetrachloride In dichloromethane at 0 - 25℃; for 6h; Acetylation;78%
29541-97-7

9-acetoxynonal

120593-09-1

((E)-Pent-3-enylidene)-triphenyl-λ5-phosphane

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

Conditions
ConditionsYield
at -78℃;62%
29541-97-7

9-acetoxynonal

53143-96-7

<(E)-3-Pentenyl>triphenylphosphonium-bromid

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

Conditions
ConditionsYield
Stage #1: <(E)-3-Pentenyl>triphenylphosphonium-bromid With sodium hexamethyldisilazane In tetrahydrofuran at -78℃; for 1h; Inert atmosphere;
Stage #2: 9-acetoxynonal In tetrahydrofuran at -78 - 20℃; for 24h; Inert atmosphere;
56%
Stage #1: <(E)-3-Pentenyl>triphenylphosphonium-bromid With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -20℃; for 1h;
Stage #2: 9-acetoxynonal In tetrahydrofuran; hexane at -60 - 20℃; Wittig reaction; Further stages.;
54%
42521-46-0

Tetradeca-cis-9,trans-12-dien-1-ol

108-24-7

acetic anhydride

30507-70-1

Tetradec-9Z,12E-dien-1-yl Acetate

Conditions
ConditionsYield
With pyridine Yield given;
With sodium acetate In neat (no solvent)
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  • (9Z,12E)-9,12-Tetradecadien-1-ol acetate CAS No.30507-70-1

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    (9Z,12E)-9,12-Tetradecadien-1-ol acetate CAS No.30507-70-1

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  • 9,12-Tetradecadien-1-ol,1-acetate, (9Z,12E)-

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    30507-70-1

    9,12-Tetradecadien-1-ol,1-acetate, (9Z,12E)-

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  • 9,12-Tetradecadien-1-ol,1-acetate, (9Z,12E)-

  • Casno:

    30507-70-1

    9,12-Tetradecadien-1-ol,1-acetate, (9Z,12E)-

    Min.Order: 0

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    9,12-Tetradecadien-1-ol,1-acetate, (9Z,12E)-Appearance:Off white to slight yellow solid Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Ai

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  • 9Z,12E-Tetradecadienyl acetate

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    30507-70-1

    9Z,12E-Tetradecadienyl acetate

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  • 30507-70-1

  • Casno:

    30507-70-1

    30507-70-1

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Chemistry

Product Name: 9Z,12E-Tetradecadienyl acetate (CAS NO.30507-70-1)


Molecular Formula: C16H28O2
Molecular Weight: 252.3923 g/mol
Mol File: 30507-70-1.mol
Boiling point: 334.8 °C at 760 mmHg
Flash Point: 102.3 °C
Density: 0.89 g/cm3
Surface Tension: 30.8 dyne/cm
Enthalpy of Vaporization: 57.78 kJ/mol
Vapour Pressure: 0.000125 mmHg at 25°C
XLogP3-AA: 5.3
H-Bond Donor: 0
H-Bond Acceptor: 2

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 oral > 1gm/kg (1000mg/kg)   Japan Pesticide Information. Vol. (40), Pg. 32, 1982.
rat LD50 oral > 1gm/kg (1000mg/kg)   Japan Pesticide Information. Vol. (40), Pg. 32, 1982.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Moderately toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating vapors.

Specification

 9Z,12E-Tetradecadienyl acetate ,its CAS NO. is 30507-70-1,the synonyms is (2E,5Z)-14-Acetoxy-2,5-tetradecadiene ; (9Z,12E)-9,12-Tetradecadien-1-ol acetate ; Acetic acid (9Z,12E)-9,12-tetradecadienyl ester ; Acetic acid [(9Z,12E)-9,12-tetradecadienyl] ester ; Litlure B ; trans,cis-9,12-Tetradecadienyl acetate .