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4229-44-1

Basic Information
CAS No.: 4229-44-1
Name: N-Methylhydroxylamine hydrochloride
Article Data: 11
Cas Database
Molecular Structure:
Molecular Structure of 4229-44-1 (N-Methylhydroxylamine hydrochloride)
Formula: CH6ClNO
Molecular Weight: 83.5177
Synonyms: Hydroxylamine,N-methyl-, hydrochloride (6CI,7CI,8CI);Methanamine, N-hydroxy-, hydrochloride(9CI);Methylhydroxylamine hydrochloride;Methylhydroxylammonium chloride;N-Hydroxy-N-methanamine hydrochloride;N-Hydroxy-N-methylammonium chloride;N-Hydroxymethanamine hydrochloride;N-Methylhydroxylammonium chloride;
EINECS: 224-181-2
Density: 1.36 g/cm3
Melting Point: 86-88 °C(lit.)
Boiling Point: 69.4 °C at 760 mmHg
Flash Point: 41.9 °C
Solubility: 0.1 g/mL in water, clear, very faintly yellow
Appearance: White to almost white crystals or cryst. powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36-24/25
Transport Information: UN 1759
PSA: 32.26000
LogP: 0.78790
Synthetic route
41106-02-9

C-(2-nitrophenyl)-N-methyl-nitrone

A

4229-44-1

N-methylhydroxyamine hydrochloride

B

3717-25-7, 4836-00-4, 6635-41-2

2-nitrobenzaldehyde oxime

Conditions
ConditionsYield
With hydroxylamine hydrochloride In methanol; diethyl ether at 20℃; for 4h;A 98%
B n/a
67036-74-2, 67036-80-0

4-(N-methylnitrono)-2,2,5,5-tetramethyltetrahydrofuran-3-one E-isomer

A

14744-18-4

2,2,5,5-Tetramethyl-furan-3,4-dione

B

4229-44-1

N-methylhydroxyamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride Heating;A 46%
B 94%
With hydrogenchloride Heating;A 43%
B 94%
With hydrogenchloride Product distribution; Heating;A 43%
B 94%
75-52-5

nitromethane

4229-44-1

N-methylhydroxyamine hydrochloride

Conditions
ConditionsYield
With ammonium chloride; zinc In water for 0.5h;
With ammonium chloride; zinc In water at 0 - 15℃;
7647-01-0

hydrogenchloride

7500-79-0

N-methyl-diphenyl-nitrone

A

119-61-9

benzophenone

B

4229-44-1

N-methylhydroxyamine hydrochloride

Conditions
ConditionsYield
Hydrolysis;
80653-57-2

N,O-Dimesyl-N-methylhydroxylamin

A

110-88-3

1,3,5-Trioxan

B

50-00-0

formaldehyd

C

593-77-1

N-Methylhydroxylamine

D

4229-44-1

N-methylhydroxyamine hydrochloride

E

2386-57-4

methanesulfonic acid sodium salt

F

NH3

NH3

Conditions
ConditionsYield
With sodium hydroxide In water Mechanism; Product distribution; hydrolysis with basic, neutral and acidic aqu. solutions;A 5 % Spectr.
B n/a
C 1 % Spectr.
D n/a
E 33 % Spectr.
F n/a
314768-38-2, 919112-42-8

(Z)-C-(3,4-dimethoxyphenyl)-N-methyl-nitrone

A

2169-98-4, 39627-82-2

3,4-Dimethoxy-benzaldehyde oxime

B

4229-44-1

N-methylhydroxyamine hydrochloride

Conditions
ConditionsYield
With hydroxylamine hydrochloride In methanol; diethyl ether at 20℃; for 4h;
593-77-1

N-Methylhydroxylamine

4229-44-1

N-methylhydroxyamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In water at 25℃; Cooling with ice;333.4 g
4229-44-1

N-methylhydroxyamine hydrochloride

555-16-8

4-nitrobenzaldehdye

16089-71-7, 57414-31-0, 97792-07-9

N-(p-nitrobenzylidene)methylamine N-oxide

Conditions
ConditionsYield
With 3 A molecular sieve at 20℃; for 0.25h;100%
With sodium hydroxide; silica gel at 20℃; for 0.166667h;96%
With sodium hydrogencarbonate In dichloromethane for 0.1h; microwave irradiation;95%
4229-44-1

N-methylhydroxyamine hydrochloride

552-89-6

2-nitro-benzaldehyde

41106-02-9

α-(2-nitrophenyl)-N-methylnitrone

Conditions
ConditionsYield
With 3 A molecular sieve at 20℃; for 0.25h;100%
With sodium hydroxide; silica gel at 20℃; for 0.166667h;98%
With potassium carbonate In methanol Reflux;96.5%
With ethanol; potassium acetate
4229-44-1

N-methylhydroxyamine hydrochloride

88176-86-7

3a-(3,4-dimethoxyphenyl)-5,5-(ethylenedioxy)-3,3a,4,5,6,7-hexahydro-2H-inden-2-one

91713-15-4

3a-(3,4-dimethoxyphenyl)-5,5-(ethylenedioxy)-3,3a,4,5,6,7-hexahydro-2H-inden-2-one N-methylnitrone

Conditions
ConditionsYield
With sodium acetate In ethanol for 40h; Heating;100%
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hydron; N-methylhydroxylamine; chloride

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Chemistry

Molecular Formula: CH6ClNO
Molecular Weight: 83.52
EINECS: 224-181-2
Polar Surface Area: 12.47 Å2
Flash Point: 41.9 °C 
Sensitive  Hygroscopic
Melting Point: 86-88 °C(lit.)
Enthalpy of Vaporization: 36.27 kJ/mol 
Boiling Point: 69.4 °C at 760 mmHg 
Vapour Pressure: 96.6 mmHg at 25°C 
IUPAC Name: N-methylhydroxylamine hydrochloride                             
Solubility: H2O: 0.1 g/mL, clear, very faintly yellow
Water Solubility of N-Methylhydroxylamine hydrochloride (CAS NO.4229-44-1): soluble
Synonyms of N-Methylhydroxylamine hydrochloride (CAS NO.4229-44-1): Methanamine,n-hydroxy-,Hydrochloride ; N-hydroxy-methanaminhydrochloride ; N-methylhydroxyaminehydrochloride ; Hydroxylaminomethane hydrochloride ; N-methylhydroxylamine hcl ; N-methylhydroxylamine hydrochloride ; N-methylhydroxylammonium chloride ; N-methylhydroxylaminehydrochloride,98%                                        
Following is the molecular structure of N-Methylhydroxylamine hydrochloride (CAS NO.4229-44-1):

Safety Profile

Safety Information of N-Methylhydroxylamine hydrochloride (CAS NO.4229-44-1):
Hazard Codes: Xi
Xi: Irritant
Risk Statements: 36/37/38
36/37/38: Irritating to eyes, respiratory system and skin 
Safety Statements: 26-36-24/25
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing 
24/25:  Avoid contact with skin and eyes 
RIDADR: 1759
WGK Germany: 3