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602-38-0

Basic Information
CAS No.: 602-38-0
Name: 1,8-Dinitronaphthalene
Article Data: 56
Cas Database
Molecular Structure:
Molecular Structure of 602-38-0 (1,8-Dinitronaphthalene)
Formula: C10H6 N2 O4
Molecular Weight: 218.169
Synonyms: 1,8-Dinitronaphthalene;NSC 6323
EINECS: 210-016-1
Density: 1.481g/cm3
Melting Point: 171 - 172 C (97 %)
Boiling Point: 389.8°C at 760 mmHg
Flash Point: 200.3°C
Solubility: 0.1 g/100ml AUTOIGNITION Yellow Crystalline Powder
Hazard Symbols: UN NO.
Risk Codes: 11-36/37/38
Safety:
Transport Information: 25kgs
PSA: 91.64000
LogP: 3.70260
Synthetic route
518-05-8

Naphthalene-1,8-dicarboxylic acid

602-38-0

1,8-dinitronaphthalene

Conditions
ConditionsYield
With nitronium tetrafluoborate; silver carbonate In N,N-dimethyl acetamide at 90℃; for 12h; Inert atmosphere; Schlenk technique; regioselective reaction;81%
91-20-3

naphthalene

A

86-57-7

1-Nitronaphthalene

B

602-38-0

1,8-dinitronaphthalene

C

605-71-0

1,5-dinitronaphthalene

Conditions
ConditionsYield
With nitric acid at 64.84℃; for 3h; Catalytic behavior; Reagent/catalyst;A 78.5%
B 10.6%
C 6.2%
With nitric acid In acetic acid at 64.84℃; for 3h; Catalytic behavior; Solvent;A 22.5%
B 42.5%
C 32.6%
With phosphotungstic acid; nitric acid at 64.84℃; for 3h; Catalytic behavior; Reagent/catalyst;A 31.5%
B 36.7%
C 28.5%
With nitric acid In dichloromethane for 12h; Reflux; regioselective reaction;
91-20-3

naphthalene

A

602-38-0

1,8-dinitronaphthalene

B

605-71-0

1,5-dinitronaphthalene

Conditions
ConditionsYield
With nitric acid at 64.84℃; for 3h; Catalytic behavior; Reagent/catalyst;A 49.2%
B 48.5%
With nitric acid
With nitric acid Erwaermen des Reaktionsgemischs mit konz. Schwefelsaeure;
91-20-3

naphthalene

602-38-0

1,8-dinitronaphthalene

Conditions
ConditionsYield
With sulfuric acid; nitric acid
With Nitrogen dioxide
86-57-7

1-Nitronaphthalene

602-38-0

1,8-dinitronaphthalene

Conditions
ConditionsYield
With sulfuric acid; potassium nitrate at 0℃;
With sulfuric acid; nitric acid at 0 - 35℃;
With sulfuric acid; nitric acid
86-57-7

1-Nitronaphthalene

A

602-38-0

1,8-dinitronaphthalene

B

605-71-0

1,5-dinitronaphthalene

Conditions
ConditionsYield
With nitric acid
With sulfuric acid; nitric acid at 0℃; Trennung der beiden Isomere durch Umkrystallisieren aus Pyridin;
With sulfuric acid; nitric acid at 0℃;
90765-71-2

1-amino-4,5-dinitronaphthalene

602-38-0

1,8-dinitronaphthalene

Conditions
ConditionsYield
With sulfuric acid; acetic acid Diazotization.Behandlung der Diazoniumsalz-Loesung mit Cu2O und Aethanol;
99972-07-3

4,5-dinitro-[1]naphthoic acid

142-71-2

copper diacetate

602-38-0

1,8-dinitronaphthalene

91-20-3

naphthalene

A

602-38-0

1,8-dinitronaphthalene

B

24824-25-7

1,7‑dinitronaphthalene

C

607-46-5

1,6-dinitronaphthalene

D

605-71-0

1,5-dinitronaphthalene

Conditions
ConditionsYield
With cupric nitrate trihydrate supported on K 10 montmorillonite clay; nitric acid; acetic anhydride In tetrachloromethane for 3h; Ambient temperature; Yield given. Yields of byproduct given;
91-20-3

naphthalene

A

86-57-7

1-Nitronaphthalene

B

602-38-0

1,8-dinitronaphthalene

C

606-37-1

2,4-dinitronaphthalene

D

581-89-5

2-nitronaphthalene

E

605-71-0

1,5-dinitronaphthalene

Conditions
ConditionsYield
With Nitrogen dioxide; ozone In dichloromethane at -25℃; for 0.0833333h; Product distribution; Mechanism; other methylnaphthalenes; also with HNO3/Ac2O system and with methanesulfonic acid; var. temp. and reaction times;
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Chemistry

Chemical Name: 1,8-Dinitronaphthalene
IUPAC NAME: 1,8-Dinitronaphthalene
CAS No.: 602-38-0
EINECS: 210-016-1
RTECS: QJ4552000
RTECS Class: Mutagen
Molecular Formula: C10H6N2O4
Molecular Weight: 218.17 g/mol
Melting Point: 161 °C
Density: 1.481 g/cm3
Flash Point: 200.3 °C
Boiling Point: 389.8 °C at 760 mmHg
Following is the structure of 1,8-Dinitronaphthalene (CAS No.602-38-0):


The chemical synonymous of 1,8-Dinitronaphthalene (CAS No.602-38-0) are 1,8-Dinitro-Naphthalen ; 1,8-Dinitronaphthalene ; Labotest-Bb Lt00436938 ; 1,8-Dinitronaphthalene, Contains Variable Amounts Of Water, 97% ; Naphthalene, 1,8-Dinitro- ; 1,8-Dinitronaphthalene,85%

Toxicity Data With Reference

1.    

mmo-sat 100 µg/plate

    MUREAV    Mutation Research. 91 (1981),321.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Suspected carcinogen. Mutation data reported. When heated to decomposition it emits toxic vapors of NOx.
Attention:
1. Storage: Store in a cool, dry place. Store in a tightly closed container.
2. Handling: Use spark-proof tools and explosion proof equipment. Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes.

Standards and Recommendations

DFG MAK: Confirmed Animal Carcinogen with Unknown Relevance to Humans