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90-44-8

Basic Information
CAS No.: 90-44-8
Name: Anthrone
Article Data: 164
Cas Database
Molecular Structure:
Molecular Structure of 90-44-8 (Anthrone)
Formula: C14H10O
Molecular Weight: 194.233
Synonyms: Anthrone(6CI,8CI);9-Oxoanthracene;Anthracene, 9,10-dihydro-9-oxo-;Carbothrone;NSC1965;
EINECS: 201-994-0
Density: 1.194 g/cm3
Melting Point: 152-157 ºC
Boiling Point: 343.4 ºC at 760 mmHg
Flash Point: 150.3 ºC
Solubility: insoluble in water
Appearance: off-white to light yellow crystals
Hazard Symbols: IrritantXi,HarmfulXn
Risk Codes: 36/37/38-20/21/22
Safety: 26-36
Transport Information: N/A
PSA: 17.07000
LogP: 2.82180
Synthetic route
612-35-1

2-Benzylbenzoic acid

90-44-8

anthracen-9(10H)-one

Conditions
ConditionsYield
With pyrophosphoryl chloride at 20℃; for 0.5h;100%
With 2C2H3F3O*BF3 In dichloromethane Friedel-Crafts acylation;100%
With Nafion-H In various solvent(s) at 180℃; for 2h; Acylation; Friedel-Crafts intramolecular acylation;92%
96913-94-9

9,10-bis(trimethylsilyl)-9,10-dihydro-9,10-epoxyanthracene

90-44-8

anthracen-9(10H)-one

Conditions
ConditionsYield
With trifluoroacetic acid In chloroform-d1 for 0.0833333h;100%
92560-84-4

anthracen-9(10H)-one oxime

90-44-8

anthracen-9(10H)-one

Conditions
ConditionsYield
With dihydrogen peroxide; tripropylammonium fluorochromate (VI) In acetone at 0 - 10℃; for 6.5h;97%
With CuCl*Kieselghur; oxygen In dichloromethane at 20℃; for 0.5h;85%
613-31-0

9,10-dihydroanthracene

[(C12H8N2)2Mn(μ-O)2Mn(C12H8N2)2](ClO4)4

A

100685-12-9, 463965-74-4

[(1,10-phenanthroline)2Mn(η1-OClO3)2]

B

120-12-7

anthracene

C

90-44-8

anthracen-9(10H)-one

D

84-65-1

9,10-phenanthrenequinone

Conditions
ConditionsYield
In acetonitrile Kinetics; the soln. in acetonitrile was allowed to stand overnight at room temp.; the organic products were detected by GC/MS; the soln. was layered with ether;A n/a
B 97%
C 0.8%
D 2%
613-31-0

9,10-dihydroanthracene

90-44-8

anthracen-9(10H)-one

Conditions
ConditionsYield
With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; cobalt(II) diacetate tetrahydrate In dichloromethane; water at 0 - 5℃; for 6h; pH=8.3;96%
With manganese(IV) oxide at 105℃; for 0.0416667 - 0.0666667h; Inert atmosphere; Microwave irradiation;90%
With tert.-butylhydroperoxide; 0.5C34H18N16(4-)*2H2O*2Cu(1+)*C3H7NO In water at 20℃; for 4h; Reagent/catalyst; Sonication;87%
611-63-2

9,10-dihydroanthracen-9-ol

90-44-8

anthracen-9(10H)-one

Conditions
ConditionsYield
With dihydrogen peroxide In water; acetonitrile at 25℃; for 1.58333h;96%
With tert.-butylnitrite; oxygen; 3,6-di(2'-pyridyl)-1,2,4,5-tetrazine; acetic acid In acetonitrile at 20℃; for 4.5h; Irradiation;87%
With ammonium nitrate; hydrogenchloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In water; acetonitrile at 60℃; for 6h; Green chemistry;82%
1499-12-3

9-acetoxyanthracene

90-44-8

anthracen-9(10H)-one

Conditions
ConditionsYield
With porcine liver esterase In aq. phosphate buffer; dimethyl sulfoxide at 37℃; for 1h; pH=7.5; Reagent/catalyst; Enzymatic reaction;94%
611-63-2

9,10-dihydroanthracen-9-ol

A

120-12-7

anthracene

B

90-44-8

anthracen-9(10H)-one

C

84-65-1

9,10-phenanthrenequinone

Conditions
ConditionsYield
With aluminum oxide; Ru(OH)x; oxygen In para-xylene at 129.85℃; under 760 Torr; for 0.166667h;A 91%
B 7%
C 2%

C24H20O

A

90-44-8

anthracen-9(10H)-one

B

118620-70-5

1,5-cyclodecadiyne

Conditions
ConditionsYield
With potassium hydride In tetrahydrofuran at 25℃; for 0.5h;A n/a
B 90%
132556-02-6

Anthronesemicarbazone

90-44-8

anthracen-9(10H)-one

Conditions
ConditionsYield
With potassium permanganate; silica gel In water at 20℃; for 0.25h;88%
With barium permanganate In acetonitrile for 4h; Heating;51%
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Consensus Reports

 Anthrone (CAS NO.90-44-8) is reported in EPA TSCA Inventory.

Specification

1.Introduction of Anthrone

The Anthrone, with its CAS NO 90-44-8, is a kind of off-white to light yellow crystals. It has synonyms of Anthrone(6CI,8CI);9-Oxoanthracene;Anthracene, 9,10-dihydro-9-oxo-;Carbothrone and NSC1965. Anthrone should be stored in a cool, dry place and in a tightly closed container. It is mainly used for a popular cellulose assay and in the colorometric determination of carbohydrates.

2.Properties of Anthrone

(1) Molecular Weight: 194.2286  (2) IUPAC Name: 10H-anthracen-9-one  (3) Appearance: off-white to light yellow crystals
(4) Nominal Mass: 194 Da  (5) Average Mass: 194.2286 Da  (6) Monoisotopic Mass: 194.073165 Da
(7) Index of Refraction: 1.639  (8) Molar Refractivity: 58.53 cm3  (9) Molar Volume: 162.5 cm3
(10) Surface Tension: 48.7 dyne/cm  (11) Density: 1.194 g/cm3  (12) Flash Point: 150.3 °C
(13) Enthalpy of Vaporization: 58.72 kJ/mol  (14) Boiling Point: 343.4 °C at 760 mmHg (15) Vapour Pressure: 7.07E-05 mmHg at 25°C
 

3.Structure descriptors of Anthrone

IUPAC Name: 10H-anthracen-9-one

InChI: InChI=1S/C14H10O/c15-14-12-7-3-1-5-10(12)9-11-6-2-4-8-13(11)14/h1-8H,9H2

InChIKey: RJGDLRCDCYRQOQ-UHFFFAOYSA-NCanonical SMILES : C1C2=CC=CC=C2C(=O)C3=CC=CC=C31
 

4.Safety information of Anthrone

Hazard Codes: HarmfulXnIrritantXi
Risk Statements: 36/37/38-20/21/22
R36/37/38: Irritating to eyes, respiratory system and skin
R20/21/22: Harmful by inhalation, in contact with skin and if swallowed
Safety Statements: 26-36
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S36: Wear suitable protective clothing
WGK Germany: 3
RTECS: CB8925500
F: 8
Mutation data reported. When heated to decomposition it emits acrid smoke and irritating vapors.